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首页>《中国测试》期刊>本期导读>烟丝含水率对成品烟丝致香成分影响的研究

烟丝含水率对成品烟丝致香成分影响的研究

108    2019-07-26

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作者:李达1, 李晓科1, 许仁杰1, 袁鹏1, 李娥贤2

作者单位:1. 红云红河烟草(集团)有限责任公司, 云南 昆明 650231;
2. 云南省农业科学研究院生物技术与种质资源研究所, 云南 昆明 650223


关键词:卷烟烟丝;薄板干燥;致香成分;自动化


摘要:

为研究薄板干燥工序中不同含水率对同一规格不同批次卷烟试样烟丝样品中致香物质的组成及含量的影响,建立静态顶空-气相色谱质谱(HS-GC/MS)联用法,以乙酸-2-苯乙酯为内标,MES自动控制系统采集数据,结合NIST和WILEY谱库检索定性、内标定量,对国内市售卷烟品牌R的两个不同批次(E、F)样品中致香成分进行测定。两个批次的成品烟丝共检测出41种核心致香成分,其中批次E含39种,批次F含37种;6-甲基-3,5-庚二烯-2-酮、六氢金合欢基丙酮为E中未检出的成分,2-(2-戊烯基)呋喃、氧化异佛尔酮、二氢猕猴桃内酯和苯乙烯为F中未检出的成分;E中的致香物质相对总含量小于样品F中的致香物质相对总含量,将薄板干燥工序烟丝含水率控制在14%有利于保存烟丝中的致香成分。静态顶空结合MES系统可以快速准确对样品进行分析测定,条件温和,操作简单,数据获取自动化、智能化,有利于提高生产质量,在烟草行业的生产制造方面具有积极影响。


Study on the influence of different moisture content on the aroma components of finished tobacco in cigarettes
LI Da1, LI Xiaoke1, XU Renjie1, YUAN Peng1, LI Exian2
1. Hongyun Honghe Tobacco (Group) Co., Ltd., Kunming 650231, China;
2. Institute of Biotechnology and Genetic Resources, Yunnan Academy of Agricultural Sciences, Kunming 650223, China
Abstract: To study the effects of different moisture content on the composition and content of aroma components in test samples of different batches of cigarettes of the same specification. A static headspace-gas chromatography-mass spectrometry (HS-GC/MS) method was established. The reaction was performed with-2-ethyl acetate as the internal standard. The data was collected by the MES automatic control system. The NIST and WILY libraries were used to search the qualitative and internal standards. Quantitatively, the aroma components in two different batches (E, F) of the domestic commercial cigarette brand R were measured. Atotal of 41 core aroma components were detected in two batches of finished cut tobacco, of which batch E contained 39 and batch F contained 37; 6-methyl-3,5-heptadien-2-one, Hexahydrofarnesyl acetone are undetected components in E, 2-(2-pentenyl) furan, isofordone oxide, dihydroactinidioli and styrene are undetected components in F; the relative total content of aroma substances in E is less than the relative total content of aroma substances in sample F, and controlling the moisture content of the drying process of thin plate at 14% is favorable to keep the aroma components in the tobacco. The static headspace combined with MES system can quickly and accurately analyze and determine samples. The conditions are mild, the operation is simple, the data acquisition is automated, intelligent, and it is conducive to improving production quality. It has a positive impact on the manufacturing of the tobacco industry.
Keywords: cigarette cut tobacco;drying process of thin plate;aroma component;automation
2019, 45(7):74-79  收稿日期: 2019-02-06;收到修改稿日期: 2019-03-25
基金项目: 红云红河烟草(集团)有限责任公司科技项目(HYHH2016GY04)
作者简介: 李达(1980-),男,云南红河州人,工程师,硕士,主要从事烟草化学、信息化研究
参考文献
[1] 段胜智, 李军营, 杨利云, 等. 烟叶致香成分及其环境影响因子的研究进展[J]. 贵州农业科学, 2015, 43(1):45-52
[2] 叶贤文,谢学云,孟韦名,等. 采收成熟度对烤烟致香物质和感官质量的影响[J]. 昆明学院学报, 2019, 41(3):15-19
[3] 黎洪利, 文鹏, 戴迎雪, 等. 烟支含水率对卷烟烟气成分的影响[J]. 中国烟草学报, 2009, 15(2):10-14
[4] 王宝兴, 毕勇, 李忠, 等. 云南烤烟中挥发性物质的系统研究[A]. CORESTA大会文集, 1996.
[5] 常爱霞, 贾兴华, 郝廷亮, 等. 特香型烤烟挥发性致香物质的测定与分析[J]. 中国烟草科学, 2002(1):1-5
[6] 景延秋, 宫长荣, 张月华, 等. 烟草香味物质分析研究进展[J]. 中国烟草科学, 2005(2):44-48
[7] 李鹏, 吴鸣, 谢剑平. 白肋烟中一些重要碱性成分和羰基化合物的分析研究[J]. 中国烟草学报, 2002, 8(1):1-5
[8] 马挺军, 曾会明. 烟草香味物质的研究进展[J]. 农产品加工(创新版), 2010(6):55-57
[9] 曹琳, 秦利霞, 康诗钊, 等. 香精香料的常见检测方法综述[J]. 上海应用技术大学, 2017, 45(21):17-20
[10] 黄曼艳, 陈森林, 陶红, 等. 烟叶中致香成分前处理与检测方法研究进展[J]. 食品保险质量检测学报, 2018, 9(9):2072-2079
[11] 高辉, 邱昌桂, 徐南山, 等. 不同干燥方式对烟丝加工质量的影响[J]. 云南农业大学学报, 2016, 31(1):127-135
[12] 张宏宇. 含水率对烟草燃烧性与烟气化学成分的影响[D]. 昆明:昆明理工大学, 2015.
[13] 孙雯, 李雪梅, 曾晓鹰, 等. 烟丝含水率对卷烟燃吸品质、烟气水分及粒相物挥发性成分的影响[J]. 烟草科技, 2009(11):33-39
[14] 云雪, 訾莹莹, 赖东辉, 等. 烟丝含水率对卷烟落锥及烟气成分的影响[J]. 安徽农业科学, 2017, 45(22):69-72
[15] 蒋举兴, 夏启东, 段焰青, 等. 卷烟香精香料中23种加香物质的气相色谱质谱法检测[J]. 食品工业, 2013, 34(9):221-223